skip to main content

Optimization of Soxhlet Extraction Papaya Seed Oil (Carica papaya L.) with Petroleum Ether

*Riski Andriana  -  Department of Technology Industry, Vocational School, Diponegoro University, Jl. Prof. Sudarto, SH, Tembalang, Semarang, Indonesia 50275, Indonesia
R. TD. Wisnu Broto  -  Department of Technology Industry, Vocational School, Diponegoro University, Jl. Prof. Sudarto, SH, Tembalang, Semarang, Indonesia 50275, Indonesia
Open Access Copyright 2023 Journal of Vocational Studies on Applied Research under http://creativecommons.org/licenses/by-sa/4.0.

Citation Format:
Abstract

Papaya seed oil is a high source of fatty acids, especially oleic acid, and palmitic acid. It has 71.60% oleic acid, 15.13% palmitic acid, and has a low cholesterol content so it can be useful as a food oil. This study aims to determine the effect of the ratio of ingredients, time, and particle size on the maximum extraction of papaya seed oil. Extraction of papaya seed oil was carried out by the soxhletation extraction method using petroleum ether solvent. The factorial experimental design of 23 was used to determine the significant parameters for the resulting papaya seed oil: yield, density, fatty acid content, viscosity, and water content. The most influential process variable is particle size. The most optimal papaya seed oil extraction results were obtained at a particle size of 20 mesh, an extraction time of 180 minutes, and a ratio of ingredients to the dissolution of 1:9 (35 gram500 mL). That value obtains a yield of 57.029%.

Fulltext View|Download
Keywords: papaya seed oil; factorial design; extraction;optimization

Article Metrics:

  1. Achtami, A., (2017), Studi Karakterisasi Komponen Kimia Biji Pepaya dengan Metode Padat-Cair (Leaching) Study Of The Characterization Of Chemical Papays Chemical Components With Solid-Liquid berguna untuk mengurangi gangguan jantung , obat anti amuba , serta biji buah kosme, pp.104–110
  2. Adachukwu, I., Ogbonna, A. O., & Faith, E., (2013), Phytochemical Analysis of Paw-paw (Carica papaya) Leaves, International Journal of Life Sciences Biotechnology and Pharma Research, 2(3), pp.347–350
  3. Arifulloh,. (2013), Ekstraksi Likopen dari Buah Tomat ( Lycopersicum esculentum Mill.) dengan Berbagai Komposisi Pelarut. Jurnal Berkala Saintek, 4(1), pp.15-18
  4. Azwanida., (2015), A Review on the Extraction Methods Use in Medicinal Plants, Principle, Strength, and Limitation. Journal of Medicinal & Aromatic Plants, 04(03), pp.3–8
  5. Briones-Labarca, V., Plaza-Morales, M., Giovagnoli-Vicuña, C., & Jamett, F., (2015), High hydrostatic pressure and ultrasound extractions of antioxidant compounds, sulforaphane and fatty acids from Chilean papaya (Vasconcellea pubescens) seeds: Effects of extraction conditions and methods. International Journal of Food Science and Technology, 60(1), pp.525–534
  6. Calzada, F., Yépez-Mulia, L., & Tapia-Contreras, A., (2007). Effect of Mexican medicinal plant used to treat trichomoniasis on Trichomonas vaginalis trophozoites. Journal of Ethnopharmacology, 113(2), pp.248–251
  7. Dewi, M., (2012), Pengaruh Kondisi Ekstraksi Terhadap Karakter Minyak Dari Biji Kacang Merah. Skripsi, Universitas Negeri Yogyakarta, Indonesia
  8. Irawan, B., & Jos, B., (2010), Peningkatan Mutu Minyak Nilam dengan Ekstraksi dan Destilasi Pada Berbagai Komposisi Pelarut. Seminar Rekayasa Kimia dan Proses, pp.4–5
  9. Karepu, M. G., Suryanto, E., & Momuat, L. I., (2020), Komposisi Kimia dan Aktivitas Antioksidan dari Paring Kelapa (Cocos Nucifera). Journal of Chemistry Progress, 13(1), pp.31-47
  10. Male, O. F., & Mus, M., (2010), Fraksi Heksan dan Fraksi Metanol Ekstrak Biji Pepaya Muda Menghambat Spermatogonia Mencit (Mus Musculus) Jantan, Journal of Veteriner, 11(1), pp.36–40
  11. Maretniatin, C. D., (2008), Uji potensi antifungi ekstrak etanol daun sirih merah, Skripsi Thesis, Universitas Sanata Dharma, Indonesia
  12. Marfo, E. K., Oke, O. L., & Afolabi, O. A., (1986), Chemical composition of papaya (Carica papaya) seeds. Journal of Food Chemistry, 22(4), pp.259–266
  13. Mukhtarini., (2014), Ekstraksi, Pemisahan Senyawa, dan Identifikasi Senyawa Aktif, Jurnal Kesehatan, 7(2), pp.361-367
  14. Nasir, S., Fitriyanti, F., & Kamila, H., (2009), Ekstraksi Dedak Padi Menjadi Minyak Mentah Dedak Padi (Rice-Bran Oil)dengan Menggunakan Pelarut n-Hexane dan Ethanol, Jurnal Rekayasa Sriwijaya, 18(1), pp.37–44
  15. Octavia, D. R., (2009), Uji Aktivitas Penangkap Radikal Ekstrak Petroleum Eter , Etil Asetat dan Etanol Daun Binahong (Anredera cordifolia (Tenore) Steen) dengan Metode DPPH (2,2-difenil-1-pikrihidrazil), Skripsi, 3, pp.119–121
  16. Prihatman Kemal., (2000), Teknik Budidaya Pepaya. Jurnal Pertanian, pp.1–12
  17. Purwanto, T. L. H., (2009), Optimasi volume etanol dan akuades dalam proses perkolasi daun stevia dengan aplikasi desain faktorial. Skripsi Thesis, Universitas Sanata Dharma, Indonesia
  18. Ramadhana, N., (2018), Identifikasi Potensi Lokal Pada Tumbuhan Biji Pepaya (Carica Papaya) Sebagai Obat Tradisional Masyarakat Di Kecamatan Banggae Timur. Jurnal Saintifik, 1(2), pp.95–102
  19. Rassem, H. H. A., Nour, A. H., & Yunus, R. M., (2016), Techniques For Extraction of Essential Oils From Plants: A Review. Australian Journal of Basic and Applied Sciences, 10(16), pp.117–127
  20. Rina, D., Bahri, S., & Zulnazri, Z., (2021), Ekstraksi Minyak Kacang Tanah (Peanut Oil) Dengan Pelarut Etanol Dan N-Heksan. Chemical Engineering Journal Storage, 1(1), pp.29-41
  21. Setiaji, A., Perairan, D. B., Perikanan, F., & Ilmu, D. A. N., (2009), Pencegahan dan Pengobatan Ikan Lele Dumbo Clarias sp yang Diinfeksi Bakteri Aeromonas hydrophila. Jurnal Medik Veteriner, 2(2), pp.89-95
  22. Soetjipto. H. dkk., (2018), Profil Asam Lemak dan Karakterisasi Minyak Biji Labu Kuning (Cucurbita moschata D.), Jurnal Kimia dan Kemasan, 40(2), pp.79-86
  23. Subramaniam, V. V. R. & Achaya, K. T., (1957), Lesser known Indian vegetable fats. l--Oleic rich fats. Journal of the Science of Food and Agriculture, 8(11), pp.657-662
  24. Sukadana, I., Rahayu Santi, S., & Juliarti, N., (2008), Aktivitas Antibakteri Senyawa Golongan Triterpenoid dari Biji Pepaya (Carica papaya L.), Jurnal Kimia, 2(1), pp.15–18
  25. Susanti, A. D., Ardiana, D., P, G. G., & G, Y. B., (2012), Polaritas Pelarut Sebagai Pertimbangan Dalam Pemilihan Pelarut Untuk Ekstraksi Minyak Bekatul dari Bekatul Varietas Ketan (Oriza Sativa Glatinosa). Simposium Nasional. pp.8-14
  26. Susilowati & Primaswari., (2012), Pengambilan Minyak Biji Kemiri (Aleurites moluccana) Melalui Ekstraksi dengan Menggunakan Soxhlet, Skripsi, Universitas Sebelas Maret, Indonesia
  27. Tambun, R., Limbong, H. P., Pinem, C., & Manurung, E., (2016), Fenol Dari Lengkuas Merah Influence of Particle Size , Time and Temperature To Extract Phenol. Jurnal Teknik Kimia, 5(4), pp.53–56
  28. Wulandari, R. H., (2017), Ekstraksi Minyak Biji Pepaya dengan Variasi Rasio Pelarut Terhadap Bahan dan Waktu Ekstraksi, Skripsi, Universitas Muhammadiyah Surakarta, Indonesia
  29. Ashurst, P.R,. (1995), Production and Packaging of Non-Carbonated Fruit Juices and Fruit Beverages. Blacklie Academic and Profesional, 2nd, An Aspen Publication, Gaithersburg, Maryland, pp.171-191
  30. Friedman, Z. & Reid, B., (1973), Essential fatty acids, prostaglandins, and human milk. In: Human milk, its biological and social value. (Freic, S. & Eidelman, A. I. (Eds)), Excerpta Medica, Amsterdam, Oxford, Princeton
  31. Grinter, R. J., Bobbitt, J. M., & Schwarting, A. E., (1991). introduction to chromatography, 2nd, ITB Press, Bandung, pp.252-254
  32. Harborne, J. B., (1987), Metode Fitokimia : Penuntun Cara Modern Menganalisis Tumbuhan Edisi ke-2, diterjemahkan oleh Padmawinata, K. dan Soediro, I, ITB Press, Bandung
  33. Hart, Harold, Leslie E Crame. David J. Hart., (1990), Kimia Organik. Terjemahan Seminar Setiadi Achmadi, Erlangga, Jakarta
  34. Ketaren, S., (2008), Pengantar Teknologi Minyak dan Lemak Pangan, UI Press, Jakarta
  35. McCabe, W. L., Smith, J. C., & Harriot, P., (1993), Unit Operations of Chemical Engineering, 5th ed. In Chemical Engineering Series (V), The McGraw-Hill Companies, New York
  36. Perry, R. H., (2007), Perrys Chemical Engineers' Handbook, editor Don W. Green, 8th ed, The McGraw-Hill Companies, New York
  37. Sabel, W. and Warren, J.D.F., (1973), Theory and practice of oleoresin extraction. In Proceedings of the Conference on Spices, Tropical Product Institut. London, pp.189-192
  38. Sudarmadji, S; B. Haryono dan Suhardi., (1989), Analisa Bahan Makanan dan Pertanian.edisi ke-2, Liberty, Yogyakarta.
  39. Sudarmadji. S. dkk., (2007), Analisis bahan makanan dan pertanian, edisi ke-2, Liberty, Yogyakarta
  40. Tiwari, P., BimleshKumar, Kaur, M., GurpreetKaur, & Kaur, H., (2017), Phytochemical screening and Extraction: A Review. Hepatology, International Pharmaceutica Sciencia, 1(1),pp.98-106
  41. Treybal, R. E., (1980), Mass Transfer Operation, 3th ed, Mc. Graw-Hill, Kogakusha Ltd
  42. Voight, R., (1994), Buku Pengantar Teknologi Farmasi, Edisi V,diterjemahkan oleh Soedani, N., Universitas Gadjah Mada Press, Yogyakarta, pp.572-574
  43. Warisno., (2003), Budi Daya Pepaya, Kanisius, Yogyakarta, pp.1-96
  44. BSN., (2019), Minyak goreng sawit, Sni 7709:2019, pp.1–28
  45. Departemen Kesehatan RI., (2000), Parameter Standar Umum Ekstrak Tanaman Obat, Buku Parameter Standar Umum, DepKes RI, Jakarta, Indonesia, pp. 10–11
  46. SmartLab., (2017), Lembar Data Keselamatan Bahan Petroleum Ether, Phase Equilibria in Binary Halides, 1907, pp.1–11

Last update:

No citation recorded.

Last update:

No citation recorded.