Synthesis and Characterization of Bi13B0.48V0.49-xPxO21.45 and Efficient Catalyst for the Synthesis of 2,3-dihydroquinazolin-4(1H)-ones Derivatives Synthesis

*Hanane Barebita scopus  -  Laboratory of Organic, Inorganic Chemistry, Electrochemistry and Environment, Faculty of Science, University of Ibn Tofail, Morocco
Youssef Merroun  -  Laboratory of Organic, Inorganic Chemistry, Electrochemistry and Environment, Faculty of Science, University of Ibn Tofail, Morocco
Soumya Ferraa scopus  -  Laboratory of Organic, Inorganic Chemistry, Electrochemistry and Environment, Faculty of Science, University of Ibn Tofail, Morocco
Abderrazak Nimour scopus  -  Laboratory of Organic, Inorganic Chemistry, Electrochemistry and Environment, Faculty of Science, University of Ibn Tofail, Morocco
Abdelaziz Souizi  -  Laboratory of Organic, Inorganic Chemistry, Electrochemistry and Environment, Faculty of Science, University of Ibn Tofail, Morocco
Taoufiq Guedira scopus  -  Laboratory of Organic, Inorganic Chemistry, Electrochemistry and Environment, Faculty of Science, University of Ibn Tofail, Morocco
Received: 20 Oct 2020; Revised: 2 Dec 2020; Accepted: 3 Dec 2020; Published: 28 Dec 2020; Available online: 19 Dec 2020.
Open Access Copyright (c) 2020 Bulletin of Chemical Reaction Engineering & Catalysis
License URL: http://creativecommons.org/licenses/by-sa/4.0

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Abstract

A new compound has been found in the system Bi13B0.48V0.49-x PxO21.45 (with 0≤x≤0.34), were prepared by the direct solid-state reaction of Bi2O3, (NH4)2HPO4, V2O5, and B2O3. This material melts congruently and it crystallize with the sillenite structure (space group I23) and form a solid solution with the cubic lattice parameter increasing from with a = 10.1568 Å to 10.1436 Å with increasing of P2O5 molar. Consequently, the new composites belong to g-variety of solid state. The samples have been characterized by Fourier transform infrared spectroscopy (FT-IR), diffraction XRD and scanning electron microscopy (SEM) coupled to the EDX. On the other hand, the valorization of the prepared composites was performed by using them as heterogeneous catalyst in the 2,3-dihydroquinazolin-4(1H)-ones derivatives synthesis. The catalyst is stable (as a bench top catalyst) and reusable. Copyright © 2020 BCREC Group. All rights reserved

 

Keywords: Bi13B0.48V0.49-x PxO21.45; Heterogeneous catalyst; 2,3-dihydroquinazolin-4(1H)-ones; γ-Bi2O3; Solid state
Funding: University of Ibn Tofail

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