Negative Effect of Calcination to Catalytic Performance of Coal Char-loaded TiO2 Catalyst in Styrene Oxidation with Hydrogen Peroxide as Oxidant

Mukhamad Nurhadi; Ratna Kusumawardani; Hadi Nur

doi:10.9767/bcrec.13.1.1171.113-118

DOI: https://doi.org/10.9767/bcrec.13.1.1171.113-118

Negative Effect of Calcination to Catalytic Performance of Coal Char-loaded TiO2 Catalyst in Styrene Oxidation with Hydrogen Peroxide as Oxidant

Mukhamad Nurhadi¹

, Ratna Kusumawardani¹, Hadi Nur²

¹Department of Chemical Education, Universitas Mulawarman, Kampus Gunung Kelua, Samarinda, 75119, East Kalimantan, Indonesia

²Centre for Sustainable Nanomaterials, Ibnu Sina Institute for Scientific and Industrial Research, Universiti Teknologi Malaysia, 81310 UTM Skudai, Johor, Malaysia

Received: 20 Apr 2017; Revised: 8 Sep 2017; Accepted: 8 Sep 2017; Available online: 22 Jan 2018; Published: 2 Apr 2018.

Editor(s): Istadi Istadi

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Abstract

The research of negative effect of calcination to catalytic performance of coal char-loaded TiO₂ catalyst in styrene oxidation with hydrogen peroxide as oxidant has successfully done. The effects of calcination step to catalyst properties were characterized with Fourier Transform Infra Red (FTIR), X-ray Difraction (XRD), nitrogen adsorption, Field Emission Scanning Electron Microscopy (FESEM), and Transmission electron microscopy (TEM). The catalytic performance of the catalysts has been investigated in styrene oxidation with hydrogen peroxide as oxidant. The catalytic study showed the calcination step influenced to catalytic properties and could decrease the catalytic performance of coal char-loaded TiO₂ catalyst in styrene oxidation.

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Keywords: Styrene; Oxidation; Calcination; Hydrogen peroxide

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Section: Original Research Articles

Language : EN

In 2018: BCREC Volume 13 Issue 1 Year 2018 (April 2018)

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